Application of Haar and Mexican Hat Wavelets to Double Divisor-Ratio Spectra for the Multicomponent Determination of Ascorbic Acid, Acetylsalicylic Acid and Paracetamol in Effervescent Tablets
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چکیده
A determinação simultânea de ácido ascórbico (AA), ácido acetilsalicílico (ASP) e paracetamol (PAR) em misturas sintéticas e tabletes efervescentes foi realizada usando-se as técnicas de transformações de Haar e transformações de onda pequena tipo chapéu mexicano (HAAR-CWT e MEXH-CWT, respectivamente), juntamente com a técnica de divisor duplo. Os métodos de processamento de sinal são baseados na aplicação de HAAR-CWT e MEXH-CWT aos espectros relativos com divisor duplo (DDRS). Estes espectros foram obtidos pela divisão do espectro de absorção do composto puro e suas misturas ternárias, por um divisor duplo ou espectro padrão correspondente à mistura de dois compostos em mistura ternária. O uso combinado de HAARCWT e MEXH-CWT com espectros relativos com divisor duplo (DDRS) foi denominado DDRSHAAR CWT e DDRS-MEXH CWT. Para avaliar a habilidade ou aplicabilidade dos métodos desenvolvidos DDRS-CWT, foi aplicado como comparação, o método espectrofotométrico por derivada de espectros relativos com divisor duplo (DDRS-DS), às amostras mencionadas acima, contendo AA, ASP e PAR. Resultados satisfatórios foram obtidos.
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تاریخ انتشار 2008